EXTRACTION OF TITANIUM DIOXIDE (TiO2) FROM IRON SAND OF TEMBAKAK BEACH WEST COAST AS NANOPARTICLES USING HYDROMETALLURGY METHOD

Lisa Rahmawati; Sudibyo; Dian Septiani  Pratama; Zipora  Sembiring; Suharso Suharso; Tika  Anggraeni; Sarwan Sarwan

doi:10.23960/analit.v9i01.165

Authors

Lisa Rahmawati Universitas Lampung
Sudibyo Badan Riset dan Inovasi Nasional (BRIN)
Dian Septiani Pratama Department of Chemistry, FMIPA, University of Lampung, Jl. Prof. Dr. Ir. Sumantri Brojonegoro No.1 Gedong Meneng, Rajabasa Bandar Lampung, Lampung 35145
Zipora Sembiring Department of Chemistry, FMIPA, University of Lampung, Jl. Prof. Dr. Ir. Sumantri Brojonegoro No.1 Gedong Meneng, Rajabasa Bandar Lampung, Lampung 35145
Suharso Suharso Department of Chemistry, FMIPA, University of Lampung, Jl. Prof. Dr. Ir. Sumantri Brojonegoro No.1 Gedong Meneng, Rajabasa Bandar Lampung, Lampung 35145
Tika Anggraeni BRIN Cibinong, Jl. Raya Jakarta-Bogor, KM 46, Cibinong, Bogor Regency, West Java
Sarwan Sarwan PT. Surveyor Carbon Consulting Indonesia, Jl. Lieutenant General R. Suprapto No. 89, RT.10/RW.04, Ramanuju, Purwakarta District, Cilegon City, Banten 42437

DOI:

https://doi.org/10.23960/analit.v9i01.165

Keywords:

Concentration, Extraction, Hydrometallurgy

Abstract

The iron sand sample came from Tembakak Beach, Pesisir Barat Regency, was prepared and then analyzed using XRF, obtained an Fe content of 58.294%; Si 18.525%; Ti 8.775%; Al 6.785%; Ca 3.885%; K 1.624%, as well as minor elements with a content below 0.5%. Titanium dioxide (TiO₂) can be obtained from ilmenite (FeTiO₃), by hydrometallurgical extraction methods. The extraction results were analyzed using XRF, obtained TiO₂ at varying concentrations of HCl 7 Îœ of 15.033%, HCl 9 Îœ of 16.367%, and HCl 12 Îœ of 17.421%. XRD characterization of TiO₂ extraction results with variations in HCl concentration of 12 Îœ shows that TiO₂ has a rutile crystal phase with a tetragonal crystal structure, and has a particle size of 33.92 nm so that the TiO₂ particles obtained are nanoparticles that play an important role in technological and industrial development.

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